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Beilstein J. Org. Chem. 2012, 8, 941–950, doi:10.3762/bjoc.8.106
Graphical Abstract
Figure 1: Important metabolites in the interaction of bacteria from the Roseobacter clade with marine algae.
Figure 2: (A) Total ion chromatogram of a headspace extract from R. pomeroyi, (B) structures of lactones rele...
Figure 3: Mass spectra of the compounds 7–11 emitted by R. pomeroyi.
Scheme 1: Synthesis of compounds 7–11. For these target structures the relative configurations are shown.
Scheme 2: Enantioselective synthesis of (2R,4S)-7 and (2S,4S)-8.
Figure 4: Enantioselective GC analyses for the assignment of the enantiomeric compositions of natural (2S,4R)-...
Beilstein J. Org. Chem. 2011, 7, 1697–1712, doi:10.3762/bjoc.7.200
Scheme 1: Fatty acid biosynthesis.
Figure 1: Volatile methyl esters from bacteria.
Figure 2: Compounds found in the headspace extracts of M. aurantiaca.
Figure 3: Total ion chromatograms of the headspace extract from M. aurantiaca (A), and expansions of the tota...
Figure 4: FAMEs identified in the headspace extracts from M. aurantiaca.
Figure 5: Mass spectra of (A) methyl dodecanoate (83), (B) methyl 2-methyldodecanoate (10), (C) methyl 4-meth...
Scheme 2: McLafferty fragmentation of FAMEs.
Figure 6: The functional group increment FG(n)FAME, HP-5 MS.
Scheme 3: Synthesis of FAMEs identified from M. aurantiaca.
Scheme 4: Synthesis of the γ- and (ω−3)-methyl branched FAME 114.
Figure 7: Mass spectra of tentatively identified methyl 4,8-dimethyldodecanoate (115) and methyl 8-ethyl-4-me...